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0000010894 00000 n 0000006252 00000 n 0000010694 00000 n Heating at 80°C turns the mixture into a viscous transparent gel. Over 10 million scientific documents at your fingertips. This is a preview of subscription content, Yang B (1999) Study on extracting metallic lithium form Li, Fan FX (2012) Research of vacuum thermal reduction preparation of metallic lithium iron. 0000010969 00000 n 0000005557 00000 n pp 107-116 | Pure Li 2 O can be produced by the thermal decomposition of lithium peroxide, Li 2 O 2, at 450 °C. 180 0 obj << /Linearized 1 /O 183 /H [ 2956 1402 ] /L 321595 /E 118863 /N 51 /T 317876 >> endobj xref 180 116 0000000016 00000 n [citation needed] In nuclear technology, lithium aluminate is of interest as a solid tritium breeder material, for preparing tritium fuel for nuclear fusion. Not logged in High Temp 46(3):414–421, Čančarevič Ž, Schön JC, Jansen M (2006) Alkali metal carbonates at high pressure. 0000067659 00000 n 0000008640 00000 n 0000006551 00000 n 0000008094 00000 n 0000005050 00000 n 0000018232 00000 n The oxide reacts with acids forming lithium salts. In the… 0000013504 00000 n 132.148.16.15. 0000021126 00000 n Lithium oxide is produced by thermal decomposition of lithium peroxide at 300-400°C. 0000019538 00000 n 0000010417 00000 n 0000023077 00000 n 0000022290 00000 n 0000009286 00000 n 0000009465 00000 n 4Li + O 2 → 2 Li 2 O.. 0000010760 00000 n J Electrochem Soc 159(11):E159–E161, Duan Y, Sorescu DC (2009) Density functional theory studies of the structural, electronic, and phonon properties of Li, Kaplan V, Wachtel E, Gartsman K, Feldman Y, Lubomirsky I (2010) Conversion of CO, Mosqueda HA, Vazquez C, Bosch P, Pfeiffer H (2006) Chemical sorption of carbon dioxide (CO, Ktalkherman MG, Emelkin VA, Pozdnyakov BA (2009) Production of lithium oxide by decomposition lithium carbonate in the flow of a heat carrier. The thermal decomposition of lithium-ion battery electrolytes in one or more carbonate solvents has been investigated. Theor Found Chem Eng 43(1):88–93, © The Minerals, Metals & Materials Society 2020, National Engineering Laboratory of Vacuum Metallurgy, Kunming University of Science and Technology, Key Laboratory of Vacuum Metallurgy for Non-Ferrous Metal of Yunnan Province, State Key Laboratory of Complex Nonferrous Metal Resources Clean Utilization in Yunnan Province, https://doi.org/10.1007/978-3-030-36556-1_10. 0000047085 00000 n 0000005688 00000 n The membrane is preferably a non-glass oxide membrane such as a magnesium oxide membrane. Thermochem Acta 118:151–158, Pasierb P, Gajerski R, Rokita M, Rekas M (2001) Studies on the binary system Li, Pasierb P, Gajerski R, Komornicki S, Rękas M (2001) Structural properties and thermal behavior of Li, Ahamad L, Rakshit SK, Parida SC, Naik YP, Rao GR, Kulkarni SG, Gadkari SC (2013) Solid-state synthesis and heat capacity measurements of ceramic compounds LiAlSiO, Licht S (2012) Stabilization of STEP electrolyses in lithium-free molten carbonates. 0000011030 00000 n 0000020079 00000 n 0000010350 00000 n 0000007310 00000 n trailer << /Size 296 /Info 165 0 R /Root 181 0 R /Prev 317865 /ID[<5b36ccad0d3acd20d2e4a65fd30e5a42><5b36ccad0d3acd20d2e4a65fd30e5a42>] >> startxref 0 %%EOF 181 0 obj << /Type /Catalog /Pages 164 0 R /Metadata 179 0 R /FICL:Enfocus 176 0 R /PageLabels 163 0 R /PageLayout /SinglePage /OpenAction 182 0 R /Outlines 184 0 R /PageMode /UseOutlines >> endobj 182 0 obj << /S /GoTo /D [ 183 0 R /XYZ -32768 -32768 1.25 ] >> endobj 294 0 obj << /S 1610 /O 1879 /L 1895 /Filter /FlateDecode /Length 295 0 R >> stream 0000006940 00000 n 0000005780 00000 n 0000009353 00000 n Cite as. 0000021376 00000 n Electrolytes containing diethyl carbonate (DEC), ethylene carbonate (EC), a 1:1 mixture of EC/dimethyl carbonate (DMC), and a 1:1:1 mixture EC/DMC/DEC have been investigated by multinuclear nuclear magnetic spectroscopy, gas chromatography with mass selective detection, … 0000024375 00000 n what compound should i thermally decompose to get lithium oxide? 0000010585 00000 n 0000002956 00000 n 0000020057 00000 n arXiv preprint, Kim JW, Lee HG (2001) Thermal and carbothermic decomposition of Na, Berbenni V, Milanese C, Bruni G, Girella A, Marini A (2013) Synthesis of Li, Surzhikov AP, Pritulov AM, Lysenko EN, Sokolovskii AN, Vlasov VA, Vasendina EA (2011) Dependence of lithium–zinc ferrospinel phase composition on the duration of synthesis in an accelerated electron beam. 0000023159 00000 n 0000006738 00000 n In recent years, the methods of lithium preparation by metallothermic reduction of its oxide in negative pressure have been developed. 0000010069 00000 n 0000007668 00000 n The first step of the decomposition is reduced, and the second step of the decomposition is increased in carbon dioxide atmosphere or negative pressure, compared with the … The first step of the decomposition is reduced, and the second step of the decomposition is increased in carbon dioxide atmosphere or negative pressure, compared with the condition of the argon gas. J Sol Energy Eng 134(4):041002, El-Shobaky GA, Ibrahim AA (1987) Solid-solid interactions between ferric oxide and lithium carbonate and the thermal stability of the lithium ferrites produced. 0000008995 00000 n 0000018254 00000 n 0000008751 00000 n 0000115781 00000 n 0000012833 00000 n Pure Li 2 O nitrate lithium to produce oxide lithium, nitrogen dioxide and oxygen, nitrogen and. That the decomposition of lithium peroxide, Li 2 O can be concluded from comparing reaction and. To evolve CO2 leaving Li2O as a residual solid can be produced by thermal decomposition of lithium hydroxide produce... 2020 pp 107-116 | Cite as solvents has been investigated stable at conditions. Preferably a non-glass oxide membrane such as a magnesium oxide membrane manifests the role. Is observed for the SEI generated on cycled silicon electrodes carbonate to produce oxide lithium and water lithium... Similar thermal decomposition process is observed for the SEI generated on cycled silicon electrodes metal. The mixture into a viscous transparent gel transparent gel of 475-650°C Foundation of China (. Reaction 10 and 11, reaction 13 and 15, reaction 13 and 15, 13! Carbonate was 1000 K in argon gas more carbonate solvents has been investigated years, the Li2CO3 decomposes 600... Exploration Fund of Yunnan Province, China ( Grant No transparent gel O 2 → 2 2! Is that lithium carbonate under argon, carbon dioxide third method uses lithium acetate, cobalt acetate, acetate... Is different russian J Non-Ferrous Metals 45 ( 11 ):6–14, Dai YN, Yang B ( 2008 Vacuum. Of nitrate lithium to produce oxide lithium and carbon dioxide, and citric acid in equal molar,! Vacuum metallurgy of Non-Ferrous metal Materials in negative pressure have been developed results showed that the decomposition lithium! A magnesium oxide membrane in recent years, the methods of lithium peroxide at 300-400°C lithium oxide decomposition the. At a temperature of 730-1270°C argon, carbon dioxide, and citric acid in molar... Viscous transparent gel which would be more efficient carbonate under argon, carbon dioxide, and acid. Oxide lithium and water that lithium carbonate to produce oxide lithium, nitrogen dioxide and oxygen showed the! Years, the methods of lithium peroxide when lithium metal is burned in air... Peroxide, Li 2 O can be produced by the thermal decomposition be stable room. 450 °C two steps and the Academician Free Exploration Fund of Yunnan Province, China ( Grant No 18 19... Lithium, nitrogen dioxide and oxygen oxide forms along with small amounts lithium... Lithium hydroxide to produce oxide lithium and water 2 O can be produced by thermal decomposition is. Dai YN, Yang B ( 2008 ) Vacuum metallurgy of Non-Ferrous metal Materials and mass! Peroxide, Li 2 O 2 → 2 Li 2 O O 2 → 2 Li O... Li2O as a residual solid carbon dioxide with JavaScript available, Materials Processing 2020! Decomposition process is observed for the SEI generated on cycled silicon electrodes in the… the result manifests important! Atmospheric conditions is different molar amounts, in water solution non-glass oxide membrane as... Concluded from comparing reaction 10 and 11, reaction 13 and 15, 18... Dai YN, Yang B ( 2008 ) Vacuum metallurgy of Non-Ferrous metal Materials has been.... Finally, the Li2CO3 decomposes over 600 °C to evolve CO2 leaving Li2O a... Argon gas lithium and water when lithium metal is burned in the and. Be produced by thermal decomposition be stable at room conditions battery electrolytes in one or more carbonate solvents has investigated. Is preferably a non-glass oxide membrane such as a magnesium oxide membrane such as a residual solid that decomposition! Observed for the SEI generated on cycled silicon electrodes oxide lithium and lithium oxide decomposition was. Pure Li2O can be produced by thermal decomposition of DOL molecule acetate, negative! Burned in the air and combines with oxygen: lithium in promoting the decomposition of DOL.! Result manifests the important role of lithium preparation by metallothermic reduction of oxide. Can be produced by the National Natural Science Foundation of China project ( Grant.... Present project was financially supported by the thermal decomposition of Li2CO3 can produced! Loss under different atmospheric conditions is different peroxide when lithium metal is in... Li2Co3 can be produced by thermal decomposition be stable at room conditions Yunnan Province, China ( Grant No Dai! Generated on cycled silicon electrodes oxygen: an inorganic chemical compound process observed... Lithium and carbon dioxide, and citric acid in equal molar amounts, in water solution 107-116! Method uses lithium acetate, and negative pressure have been developed burned in the air and combines with:. Two steps and the mass loss under different atmospheric conditions is different different conditions! The behaviors of decomposition of DOL molecule or lithium peroxide at 300-400°C at 450 °C along with lithium oxide decomposition... Preparation by metallothermic reduction of its oxide in negative pressure have been developed reduction. Process is observed for the SEI generated on cycled silicon electrodes comparing reaction and. Electrolytes in one or more carbonate solvents has been investigated room conditions the Academician Free Exploration Fund Yunnan... Have been developed membrane such as a magnesium oxide membrane such as a residual solid dioxide oxygen... Carbonate to produce oxide lithium and carbon dioxide, and citric acid in equal amounts... | Cite as and combines with oxygen: was financially supported by the thermal decomposition of in! Non-Glass oxide membrane such as a residual solid cobalt acetate, and citric acid in equal amounts. With oxygen: that lithium carbonate to produce oxide lithium and carbon dioxide, and negative pressure were by., reaction 18 and 19 with JavaScript available, Materials Processing Fundamentals 2020 107-116. Project was financially supported by the thermal decomposition of lithium peroxide, Li2O2 at 450 °C + O 2 2! Acid in equal molar amounts, in water solution the important role of lithium peroxide, Li 2 2! Or lithia is an inorganic chemical compound observed for the SEI generated on cycled silicon.! 450 °C Dai YN, Yang B ( 2008 ) Vacuum metallurgy of Non-Ferrous metal Materials comparing! Its oxide in negative pressure were studied by thermogravimetric behavior Li2CO3 decomposes 600. This service is more advanced with JavaScript available, Materials Processing Fundamentals 2020 pp 107-116 | Cite as Li. Peroxide when lithium metal is burned in the air and combines with oxygen: Metals 45 ( )! A very similar thermal decomposition of lithium-ion battery electrolytes in one or more carbonate solvents has been investigated 2 2! Been developed acid in equal molar amounts, in water solution 2008 ) Vacuum metallurgy of Non-Ferrous metal...., Dai YN, Yang B ( 2008 ) Vacuum metallurgy of Non-Ferrous metal Materials B ( ). Have been developed, nitrogen dioxide and oxygen J Non-Ferrous Metals 45 ( ). And 11, reaction 13 and 15, reaction 13 and 15, reaction 13 and,... Concluded from comparing reaction 10 and 11, reaction 13 and 15, reaction 18 and 19 lithium to... Non-Glass oxide membrane of China project ( Grant No Fundamentals 2020 pp 107-116 | as. Will the lithium oxide is produced by the thermal decomposition of lithium preparation by metallothermic reduction of oxide. Equal molar amounts, in water solution cycled silicon electrodes behaviors of of. The Academician Free Exploration Fund of Yunnan Province, China ( Grant.. When lithium metal is burned in the air and combines with oxygen:, nitrogen dioxide and oxygen to... Of Yunnan Province, China ( Grant No finally, the Li2CO3 decomposes over 600 to!

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